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Beilstein J. Org. Chem. 2013, 9, 1797–1806, doi:10.3762/bjoc.9.209
Graphical Abstract
Scheme 1: Previous work on direct allylic etherification of allylic alcohols.
Figure 1: Initial side product with TMHQ.
Scheme 2: Proposed pathway.
Scheme 3: Control reactions.
Scheme 4: Reaction of 21 with added Brønsted acid co-catalyst.
Scheme 5: Suggested mechanism.